Table 3 |
||||||
|
Summary of the validation parameters for the LC-MS/MS methods for the determination of residual antibiotics in water samples from a hospital in Ujjain, India |
||||||
|
Antibiotics |
Correlation coefficient r2 |
Coefficient of Variation (%RSD) |
LOD μg/l |
LOQ μg/l |
% Recovery n = 5 |
|
|
|
||||||
|
Interday n = 6 |
Intraday n = 6 |
|||||
|
|
||||||
|
Amoxicillin |
0.994 |
5.2 |
5.6 |
0.5 |
1.0 |
85 (%RSD 5.6) |
|
Ceftrixone |
0.997 |
2.1 |
1.8 |
2.5 |
5.0 |
84 (%RSD 4.1) |
|
Amikacin |
0.990 |
4.8 |
4.3 |
0.25 |
0.5 |
92 (%RSD 3.8) |
|
Ofloxacin |
0.999 |
3.1 |
2.57 |
0.01 |
0.025 |
95 (%RSD 3.7) |
|
Ciprofloxacin |
0.999 |
3.2 |
3.03 |
0.01 |
0.025 |
98 (%RSD 4.5) |
|
Norfloxacin |
0.999 |
3.4 |
3.02 |
0.01 |
0.025 |
90 (%RSD 3.2) |
|
Levofloxacin |
0.999 |
3.12 |
2.96 |
0.01 |
0.025 |
93 (%RSD 2.8) |
|
|
||||||
|
LOD: Limit of detection; LOQ: Limit of quantification |
||||||
|
Diwan et al. BMC Public Health 2010 10:414 doi:10.1186/1471-2458-10-414 |
||||||
